Atomic spectrometry 02-SPAL
The objective of the course is to provide students with the knowledge of the basis issues relating to analytical atomic spectrometry, possibilities of application thereof, its limitations and disturbances, as well as the rules underlying the operation of instruments used for the purpose of elements determination. LEARNING OUTCOMES. Following completion of the course students shall: I. The basic knowledge and understanding of emission, atomic absorption, as well as combinations thereof (atomic fluorescence) and inductively coupled plasma mass spectrometry - analytical methods used to determine elements in different objects. II. The ability to select proper the analytical method from among the entire set of available solutions (AES, ICPOES, FAAS, ETAAS, HGAAS, CVAAS, AFS and ICPMS) in order to solve a particular analytical problem (taking into account the reliability of the results, time and cost of the analysis). III. The ability to select proper calibrate an instrument. IV. Know the analytical potential of the particular methods (selectivity, limit of detection, limit of quantitation, working range). V. Be aware of occurrence of spectral, chemical, ionisation, isobaric and multiatomic interferences. VI. Skills to eliminate interferences. VII. Skills to interpret the test results and formulate proper conclusions. VIII. Know the basic definitions and terms used in analytical atomic spectrometry.
Bibliography
1) B. Welz, . Sperling, Atomic Absorption Spectrometry, Third. Completely revised Edition, J. Wiley - VCH Vrlag, GmbH, Federal Republic of Germany,1999.
2) W. Szczepaniak, Metody instrumentalne w analizie chemicznej, Wyd. Naukowe PWN, W-wa, 2002.
3) A. Cygański, Metody spektroskopowe w chemii analitycznej, Wyd. Naukowo-Techniczne, W-wa 1997.
4) D. Barałkiewicz, Aspekty metodyczne i specjacyjne oznaczania pierwiastków w wodzie metodą atomowej spektrometrii absorpcyjnej, Wyd. Naukowe UAM, Poznań 2001.
Additional information
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